Experimental Techniques: Microcrystallography
Routine service crystallography on microcrystals that cannot be measured elsewhere.
- Fast data collection (10 minutes) and good for air Sensitivity compounds.
- Micro crystal, size <3um.
- variable temperature (10k-300k)
Microcrystallography setup – Upper left: APEXII detector on 2θ arm with translation stage for changing detector-sample distance. Center, left to right: open-flow cryostat, sample holder, collimator, alignment camera, and smart shutter. Back: Bruker D8 diffractometer.